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Structure and properties of Kr–O2 condensed films

S. I. KovalenkoPhysicotechnical Institute of Low Temperatures, Academy of Sciences of the Ukrainian SSR, KharkovA. A. SolodovnikPhysicotechnical Institute of Low Temperatures, Academy of Sciences of the Ukrainian SSR, Kharkov
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Abstract

Electron diffraction studies of the structure of condensed Kr–O2 films have been carried out. Measurements were made in the temperature range 5−35 K on samples whose effective thickness varied from 30−40 to 400 Å. A considerable solubility (up to 40 mol % O2) was reported for the components on the Kr side below 35 K. This was facilitated by the closeness of the volumes corresponding to a partially oriented-disordered O2 molecule and a Kr atom. The solubility of Kr in α- and β-O2 was found to be negligible. The addition of small amounts of an inert gas initiated the formation of α′-phase which was transformed into β-modification near the sublimation temperature of O2. For Kr concentrations ≳ 10%, a decomposition into α and β phases was observed. Solutions with a γ-O2-structure were found to border the solidus line in the cases when the Kr concentration was <30%.

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