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On‐Line Radical Scavenging Detection and Characterization of Antioxidants from <i>Artemisia herba‐alba</i>

N. Dahmani-HamzaouiDépartement de Chimie, Faculté des Sciences, Université Mouloud Mammeri, Tizi Ouzou, AlgeriaSofı́a SalidoDepartamento de Química Inorgánica y Orgánica, Facultad de Ciencias Experimentales, Universidad de Jaén, ES-23071 Jaén (phone: +34-953-212743; fax: +34-953-211876)Pablo J. Linares‐PalominoDepartamento de Química Inorgánica y Orgánica, Facultad de Ciencias Experimentales, Universidad de Jaén, ES-23071 Jaén (phone: +34-953-212743; fax: +34-953-211876)Aoumeur BaâliouamerDépartement de Chimie Organique, Faculté de Chimie, Université des Sciences et de la Technologie Houari Boumediene, B.P. 32, El-Alia, Bab-Ezzouar, Alger 16111, AlgeriaJoaquı́n AltarejosDepartamento de Química Inorgánica y Orgánica, Facultad de Ciencias Experimentales, Universidad de Jaén, ES-23071 Jaén (phone: +34-953-212743; fax: +34-953-211876)
2012en
ABI

Abstract

Abstract Four caffeoylquinic acid (CQA) derivatives, 5‐ O ‐caffeoylquinic acid ( 1 ), 3,5‐di‐ O ‐caffeoylquinic acid ( 3 ), 4,5‐di‐ O ‐caffeoylquinic acid ( 4 ), and 3,4,5‐tri‐ O ‐caffeoylquinic acid ( 5 ), have been isolated from Artemisia herba‐alba growing wild in Algeria, using the on‐line HPLCDADDPPH radical‐scavenging detection technique as guidance. In the course of the purification work, the non‐frequent ( E )‐2‐( β ‐ D ‐glucopyranosyloxy)‐4‐methoxycinnamic acid ( 2 ) has also been isolated. The CQAs showed fair‐to‐good antioxidant activities determined by the DPPH . scavenging assay. The structures of the five isolated compounds were determined by spectroscopic methods. The on‐line HPLCDADDPPH technique allowed for a rapid pinpointing of antioxidants in the studied plant, accomplishing the facile guided isolation of the target molecules. Algerian A. herba‐alba could be an interesting source of natural antioxidants that deserve further work.

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