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Modulation of internal electric field in S-scheme heterojunction towards efficient photocatalytic CO2 conversion

Dongdong ChenKey Laboratory of Green and Precise Synthetic Chemistry and Applications, Ministry of Education, Anhui Province Key Laboratory of Pollutant Sensitive Materials and Environmental Remediation, Huaibei Normal University, Huaibei, 235000, Anhui, ChinaZhongliao WangKey Laboratory of Green and Precise Synthetic Chemistry and Applications, Ministry of Education, Anhui Province Key Laboratory of Pollutant Sensitive Materials and Environmental Remediation, Huaibei Normal University, Huaibei, 235000, Anhui, ChinaJinfeng ZhangKey Laboratory of Green and Precise Synthetic Chemistry and Applications, Ministry of Education, Anhui Province Key Laboratory of Pollutant Sensitive Materials and Environmental Remediation, Huaibei Normal University, Huaibei, 235000, Anhui, ChinaOlim RuzimuradovTurin Polytechnic University in Tashkent, Kichik Khalqa Yoli 17, Tashkent, 100095, UzbekistanShavkat MamatkulovTurin Polytechnic University in Tashkent, Kichik Khalqa Yoli 17, Tashkent, 100095, UzbekistanKai DaiKey Laboratory of Green and Precise Synthetic Chemistry and Applications, Ministry of Education, Anhui Province Key Laboratory of Pollutant Sensitive Materials and Environmental Remediation, Huaibei Normal University, Huaibei, 235000, Anhui, ChinaJingxiang LowHefei National Laboratory for Physical Sciences at the Microscale, University of Science and Technology of China, Hefei, 230026, Anhui, China
Materials Today Physicsjournal2023en
ABI

Аннотация

The internal electric field (IEF) inherent within a composite photocatalyst plays a pivotal role in orchestrating the photogenerated charge carrier separation. Consequently, achieving precise regulation of the IEF emerges as the keystone for optimizing photocatalytic performance. Herein, we present a demonstrative study centered around the deliberate manipulation of the IEF within a g-C 3 N 4 /In 2 S 3 step-scheme (S-scheme) heterojunction . This manipulation is deftly accomplished through the introduction of sulfur doping (S-doping) into the g-C 3 N 4 . Employing advanced techniques such as Kelvin probe force microscopy and density functional theory calculations, we substantiate that S-doping precipitates a reinforcement in IEF existing between g-C 3 N 4 and In 2 S 3 . The soundness of this proposition is fortified through in situ X-ray photoelectron spectroscopy, which unveils a pronounced augmentation in the accumulation of photogenerated electrons on the surface of g-C 3 N 4 subsequent to S-doping. This empirically substantiates the enhanced charge carrier dynamics made possible by the manipulation of the IEF within S-scheme heterojunction .

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