Eco-Friendly Approach for Graphene Oxide Synthesis by Modified Hummers Method
Néstor Méndez‐LozanoUniversidad del Valle de México, Campus Queretaro, Blvd. Juriquilla No. 1000 A Del. Santa Rosa Jáuregui, Queretaro C.P. 76230, MexicoFrancisco David Pérez-ReynosoUniversidad del Valle de México, Campus Queretaro, Blvd. Juriquilla No. 1000 A Del. Santa Rosa Jáuregui, Queretaro C.P. 76230, MexicoCarlos Alberto González-GutiérrezUniversidad del Valle de México, Campus Queretaro, Blvd. Juriquilla No. 1000 A Del. Santa Rosa Jáuregui, Queretaro C.P. 76230, Mexico
2022en
ABI
Аннотация
The aim of this study is to produce graphene oxide using a modified Hummers method without using sodium nitrate. This modification eliminates the production of toxic gases. Two drying temperatures, 60 °C and 90 °C, were used. Material was characterized by X-Ray Diffraction, Fourier Transform Infrared Spectroscopy, Raman Spectroscopy and Scanning Electron Microscopy. FTIR study shows various functional groups such as hydroxyl, carboxyl and carbonyl. The XRD results show that the space between the layers of GO60 is slightly larger than that for GO90. SEM images show a homogeneous network of graphene oxide layers of ≈6 to ≈9 nm. The procedure described has an environmentally friendly approach.
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