Sesquiterpenes and Monoterpenes from the Bark of <i>Inula </i><i>m</i><i>acrophylla</i>
Bao‐Ning SuFaculty of Pharmaceutical Sciences, University of Tokushima, Shomachi 1-78, Tokushima 770-8505, Japan, Faculty of Pharmaceutical Sciences, Tokushima Bunri University, Yamashiro-cho, Tokushima 770-8514, Japan, Faculty of Pharmaceutical Sciences, Kyoto University, Yoshida Sakyou-ku, Kyoto 606-8501, Japan, Faculty of Integrated Arts and Sciences, University of Tokushima, Jyousanjima, Tokushima 770-8502, Japan, and Academy of Sciences, Uzbekistan Institute of Botany, F. Khodzhaev, Street 32, 700143, UzbekistanYoshihisa TakaishiFaculty of Pharmaceutical Sciences, University of Tokushima, Shomachi 1-78, Tokushima 770-8505, Japan, Faculty of Pharmaceutical Sciences, Tokushima Bunri University, Yamashiro-cho, Tokushima 770-8514, Japan, Faculty of Pharmaceutical Sciences, Kyoto University, Yoshida Sakyou-ku, Kyoto 606-8501, Japan, Faculty of Integrated Arts and Sciences, University of Tokushima, Jyousanjima, Tokushima 770-8502, Japan, and Academy of Sciences, Uzbekistan Institute of Botany, F. Khodzhaev, Street 32, 700143, UzbekistanTetsuya YabuuchiFaculty of Pharmaceutical Sciences, University of Tokushima, Shomachi 1-78, Tokushima 770-8505, Japan, Faculty of Pharmaceutical Sciences, Tokushima Bunri University, Yamashiro-cho, Tokushima 770-8514, Japan, Faculty of Pharmaceutical Sciences, Kyoto University, Yoshida Sakyou-ku, Kyoto 606-8501, Japan, Faculty of Integrated Arts and Sciences, University of Tokushima, Jyousanjima, Tokushima 770-8502, Japan, and Academy of Sciences, Uzbekistan Institute of Botany, F. Khodzhaev, Street 32, 700143, UzbekistanTakenori KusumiTokushima UniversityMotoo ToriFaculty of Pharmaceutical Sciences, University of Tokushima, Shomachi 1-78, Tokushima 770-8505, Japan, Faculty of Pharmaceutical Sciences, Tokushima Bunri University, Yamashiro-cho, Tokushima 770-8514, Japan, Faculty of Pharmaceutical Sciences, Kyoto University, Yoshida Sakyou-ku, Kyoto 606-8501, Japan, Faculty of Integrated Arts and Sciences, University of Tokushima, Jyousanjima, Tokushima 770-8502, Japan, and Academy of Sciences, Uzbekistan Institute of Botany, F. Khodzhaev, Street 32, 700143, UzbekistanShigeru TakaokaFaculty of Pharmaceutical Sciences, University of Tokushima, Shomachi 1-78, Tokushima 770-8505, Japan, Faculty of Pharmaceutical Sciences, Tokushima Bunri University, Yamashiro-cho, Tokushima 770-8514, Japan, Faculty of Pharmaceutical Sciences, Kyoto University, Yoshida Sakyou-ku, Kyoto 606-8501, Japan, Faculty of Integrated Arts and Sciences, University of Tokushima, Jyousanjima, Tokushima 770-8502, Japan, and Academy of Sciences, Uzbekistan Institute of Botany, F. Khodzhaev, Street 32, 700143, UzbekistanGisho HondaFaculty of Pharmaceutical Sciences, University of Tokushima, Shomachi 1-78, Tokushima 770-8505, Japan, Faculty of Pharmaceutical Sciences, Tokushima Bunri University, Yamashiro-cho, Tokushima 770-8514, Japan, Faculty of Pharmaceutical Sciences, Kyoto University, Yoshida Sakyou-ku, Kyoto 606-8501, Japan, Faculty of Integrated Arts and Sciences, University of Tokushima, Jyousanjima, Tokushima 770-8502, Japan, and Academy of Sciences, Uzbekistan Institute of Botany, F. Khodzhaev, Street 32, 700143, UzbekistanMichiho ItoFaculty of Pharmaceutical Sciences, University of Tokushima, Shomachi 1-78, Tokushima 770-8505, Japan, Faculty of Pharmaceutical Sciences, Tokushima Bunri University, Yamashiro-cho, Tokushima 770-8514, Japan, Faculty of Pharmaceutical Sciences, Kyoto University, Yoshida Sakyou-ku, Kyoto 606-8501, Japan, Faculty of Integrated Arts and Sciences, University of Tokushima, Jyousanjima, Tokushima 770-8502, Japan, and Academy of Sciences, Uzbekistan Institute of Botany, F. Khodzhaev, Street 32, 700143, UzbekistanYoshio TakedaFaculty of Pharmaceutical Sciences, University of Tokushima, Shomachi 1-78, Tokushima 770-8505, Japan, Faculty of Pharmaceutical Sciences, Tokushima Bunri University, Yamashiro-cho, Tokushima 770-8514, Japan, Faculty of Pharmaceutical Sciences, Kyoto University, Yoshida Sakyou-ku, Kyoto 606-8501, Japan, Faculty of Integrated Arts and Sciences, University of Tokushima, Jyousanjima, Tokushima 770-8502, Japan, and Academy of Sciences, Uzbekistan Institute of Botany, F. Khodzhaev, Street 32, 700143, UzbekistanOlimjon K. KodzhimatovFaculty of Pharmaceutical Sciences, University of Tokushima, Shomachi 1-78, Tokushima 770-8505, Japan, Faculty of Pharmaceutical Sciences, Tokushima Bunri University, Yamashiro-cho, Tokushima 770-8514, Japan, Faculty of Pharmaceutical Sciences, Kyoto University, Yoshida Sakyou-ku, Kyoto 606-8501, Japan, Faculty of Integrated Arts and Sciences, University of Tokushima, Jyousanjima, Tokushima 770-8502, Japan, and Academy of Sciences, Uzbekistan Institute of Botany, F. Khodzhaev, Street 32, 700143, UzbekistanOzodbek AshurmetovFaculty of Pharmaceutical Sciences, University of Tokushima, Shomachi 1-78, Tokushima 770-8505, Japan, Faculty of Pharmaceutical Sciences, Tokushima Bunri University, Yamashiro-cho, Tokushima 770-8514, Japan, Faculty of Pharmaceutical Sciences, Kyoto University, Yoshida Sakyou-ku, Kyoto 606-8501, Japan, Faculty of Integrated Arts and Sciences, University of Tokushima, Jyousanjima, Tokushima 770-8502, Japan, and Academy of Sciences, Uzbekistan Institute of Botany, F. Khodzhaev, Street 32, 700143, Uzbekistan
2001he
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Аннотация
Eleven new sesquiterpenes (1--11) and two thymol derivatives (12, 13), along with 12 known sesquiterpenes and monoterpenes, were isolated from the bark of Inula macrophylla. Their structures were determined on the basis of spectral evidence (especially by HREIMS and 2D NMR) as well as chemical transformations. The structure of macrophyllic acid A (1) was confirmed by X-ray analysis, and the absolute configuration of 1 was determined on the basis of the appropriate chemical conversions and the application of a modified Mosher's method.
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