Мақола

Synthesis and Characterization of Magnetized Di(Pyridin-2-Yl)Amine-Copper (II) Complex and Its Catalytic Applications in Synthesis of Ynones and Amides

Saade Abdalkareem JasimMedical Laboratory Techniques Department, Al-Maarif University CollegeAli Thaeer HammidComputer Engineering Department, Imam Ja’afar Al-Sadiq UniversityWalid Kamal AbdelbassetDepartment of Health and Rehabilitation Sciences, College of Applied Medical Sciences, Prince Sattam Bin Abdulaziz UniversityMohamed HussienDepartment of Chemistry, Faculty of Science, King Khalid UniversityGulnora TillaevaDepartment of Research and Development, School of Pharmacy, Akfa UniversityAli MajdiDepartment of Building and Construction Techniques, Al Mustaqbal University CollegeGhulam YasinDepartment of Botany, Bahauddin Zakariya UniversityYasser Fakri MustafaDepartment of Pharmaceutical Chemistry, College of Pharmacy, University of Mosul

Polycyclic aromatic compoundsjournal2022en

ABI

Аннотация

Copper (II) complex immobilized on the surface of silica-coated magnetic nanoparticles functionalized with di(pyridin-2-yl)amine (Fe3O4@SiO2-di(pyridin-2-yl)amine-Cu(II)) was successfully fabricated and characterized by various analyses including FT-IR, SEM, TEM, EDX, TGA, XRD, VSM, AAS and ICP-OES techniques. The catalytic behavior of Fe3O4@SiO2-di(pyridin-2-yl)amine-Cu(II) nanocomposite was investigated in the synthesis of ynones and amides. Furthermore, the heterogeneous catalyst (Fe3O4@SiO2-di(pyridin-2-yl)amine-Cu(II)) can be easily recovered by external magnet and reused for 8 cycles without significant loss in activity. The results clearly exhibit the advantages of the present methodology, namely the low catalyst loading, high product yield, experimental simplicity, broad substrate scope and short reaction times.

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Мавзулар

Multicomponent Synthesis of Heterocycles Synthesis and Characterization of Pyrroles Nanomaterials for catalytic reactions

Идентификаторлар

DOI: 10.1080/10406638.2022.2112713

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