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EFFECT OF COMBINED PM AND AGING TREATMENT ON THE MICROSTRUCTURAL EVOLUTION AND CORROSION RESISTANCE OF NItI ALLOYS

Qusay Abdulsattar MohammedCollege of Dentistry, University of Al Maarif, Al Anbar 31001, IraqSokhiba IsrailovaDepartment of Public Health and Health Care Management, Samarkand State Medical University, Samarkand, UzbekistanAkanksha MishraDepartment of Mechanical Engineering, Sharda School of Engineering & Sciences, Sharda University, Greater Noida, IndiaRanveer SinghDepartment of Mechanical Engineering, Chandigarh University, Mohali, Punjab, IndiaFang NieDepartment of Materials Science, Nanjing University of Science and Technology, Nanjing 210094, Jiangsu, P. R. China
2026en
ABI

Аннотация

Nickel–titanium alloys produced through powder metallurgy were subjected to controlled aging treatments to examine how thermal exposure influences microstructural evolution, oxide formation, and corrosion performance. Aging at [Formula: see text]C for 1–3[Formula: see text]h progressively reduced porosity and promoted the development of intermetallic phases such as Ni 3 Ti, Ni 4 Ti 3 , and Ti 2 Ni, along with increasingly uniform TiO 2 surface layers. SEM, EDS, and XRD analyses confirmed enhanced oxide coverage and phase redistribution with longer aging durations. Electrochemical testing revealed a consistent improvement in corrosion resistance, with the 3[Formula: see text]h-aged alloy exhibiting the lowest corrosion rate and highest charge-transfer resistance. These results demonstrate that aging-induced TiO 2 formation significantly stabilizes the surface and improves biocorrosion behavior, offering an effective strategy for optimizing PM-processed NiTi alloys for biomedical applications.

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