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Tribromide Immobilized on Amino-Functionalized Magnetic Nanoparticles: A Active Magnetically Recoverable Catalyst for the Synthesis of Heterocycles

Saade Abdalkareem JasimMedical Laboratory Techniques Department, Al-Maarif University College, Al-Anbar-Ramadi, IraqZiyadulla Eshmamatovich ZhumanovDepartment of Pathological Anatomy, with a Section-Biopsy Course, Samarkand State Medical Institute, Samarkand, UzbekistanMaria Jade Catalan OpulenciaCollege of Business Administration, Ajman University, Ajman, United Arab EmiratesMustafa M. KadhimAl-Nisour University CollegeThulfeqar Ahmed HamzaMedical Laboratory Techniques Department, Al-Mustaqbal University College, Babylon, IraqShaymaa Abed HusseinHimanshu SharmaDepartment of Computer Engineering and Applications, GLA University, Mathura, IndiaAli Thaeer HammidComputer Engineering Techniques Department, Faculty of Information Technology, Imam Ja’afar Al-Sadiq University, Baghdad, Iraq

Polycyclic aromatic compoundsjournal2022en

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ABI

Annotatsiya

A novel tribromide nanocatalyst was successfully fabricated via the heterogenization of tribromide ion on the surface of silica-coated magnetic nanoparticles modified with N2,N4,N6-tris(aminomethyl)-1,3,5-triazine-2,4,6-triamin [Fe3O4@SiO2-tris(triazine-triamine)-Br3] and was well characterized by Fourier-transform infrared spectroscopy (FTIR), Scanning Electron Microscopy (SEM), Transmission Electron Microscopy (TEM), Energy Dispersive X-Ray Analysis (EDX), vibrating-sample magnetometer (VSM), X-ray diffraction analysis (XRD) and Thermogravimetric analysis (TGA) spectroscopic techniques. TEM and SEM analysis confirmed that the typical silica shell thickness was assessed to be around 20 nm. The as-fabricated Fe3O4@SiO2-tris(triazine-triamine)-Br3 nanomaterial was shown high catalytic activity in the multicomponent synthesis of highly substituted piperidines and polyhydroquinolines. Recycling experiments revealed that the Fe3O4@SiO2-tris(triazine-triamine)-Br3 could be easily recovered by a simple magnetic separation and recycled at least 7 times without deterioration in catalytic activity.

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Mavzular

Multicomponent Synthesis of Heterocycles Synthesis and Characterization of Heterocyclic Compounds Nanomaterials for catalytic reactions

Identifikatorlar

DOI: 10.1080/10406638.2022.2094422

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