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Palladium immobilized on KIT-6@NH2@BAP@HB: as highly efficient, novel, reusable, and organic–inorganic hybrid catalysts for the homoselective synthesis of 2, 3-cycloaddition, and CO cross-coupling reaction

Tareq Nayef AlRamadnehFaculty of Allied Medical Sciences, Hourani Center for Applied Scientific Research, Al-Ahliyya Amman University, Amman, JordanMagdi E. A. ZakiDepartment of Chemistry, Faculty of Science, Imam Mohammad Ibn Saud Islamic University (IMSIU), Riyadh, 11623, Saudi ArabiaZafar RakhmanovSchool of Exact Sciences, National Pedagogical University of Uzbekistan named after Nizami, Tashkent, UzbekistanAhmed AldulaimiFaculty of Pharmacy, Al-Zahrawi University, Karbala, IraqSara abdalkahar sleemanDepartment of Chemistry, College of Education, Alnoor University, Mosul, IraqRasul UsmanovDepartment of Chemistry, Urgench State University, Urgench, UzbekistanHarvinder Singh SohalDepartment of Chemistry, University Institute of Sciences, Chandigarh University, Mohali, Punjab, IndiaSobhi M. GomhaDepartment of Chemistry, Faculty of Science, Islamic University of Madinah, Madinah, 42351, Saudi Arabia

2026en

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ABI

Annotatsiya

The current work describes the successful synthesis of a mesoporous KIT-6-centered asparagine functionalized 2-hydroxybenzaldehyde-Palladium complex anchored nanocomposite. The novel materials, synthesized by a post-functionalization approach, have been characterized by FT-IR, XRD, TEM, XPS, SEM, EDX, ICP, and BET studies. The materials have been proven to be efficient heterogeneous catalysts in the synthesis of diary ethers by C O cross-coupling reaction and tetrazole synthesis through cycloaddition process under green conditions. The current methodology is advantageous in terms of simplicity of procedure, facile synthesis, high yield in short reaction time, easy magnetic isolation, and reusability of catalysts in consecutive runs with insignificant change in catalytic activity.

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Identifikatorlar

DOI: 10.1016/j.molstruc.2026.147026

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