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Nanoindentation Characterization of Mechanically Alloyed Fe-Al-Si Powders

Petr HaušildCzech Technical University in PragueJaroslav ČechCzech Technical University in PragueMiroslav Karlı́kCzech Technical University in PragueFilip PrůšaUniversity of Chemistry and Technology PraguePavel NovákUniversity of Chemistry and Technology PragueJaromı́r KopečekInstitute of Physics of the ASCR, v. v. i
Key engineering materialsbook series2018en
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The effect of processing conditions on microstructure and mechanical properties of Fe-Al-Si powders was studied by means of scanning electron microscopy, X-ray diffraction and nanoindentation. Fe-Al-Si alloy powder was prepared from pure elemental powders by mechanical alloying. Microstructure and mechanical properties of powders were characterized after various durations of mechanical alloying. Special sample preparation technique was developed allowing to characterize the properties of individual powder particles after each step of processing in a planetary ball mill. This step-by-step characterization allowed to find the optimum conditions for subsequent spark plasma sintering.

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