Electrochemical Synthesis of Polymer Complexes with Selected Metals Based on 1-Vinyl-1,2,4-triazole
S. H. SargsyanNational Polytechnic University of Armenia, 0009, Yerevan, ArmeniaT. S. SargsyanYerevan State Medical University after M. Heratsi, 0025, Yerevan, ArmeniaI. G. AgadjanyanNational Polytechnic University of Armenia, 0009, Yerevan, ArmeniaK. M. KhizantsyanNational Polytechnic University of Armenia, 0009, Yerevan, ArmeniaA. S. SargsyanYerevan State Medical University after M. Heratsi, 0025, Yerevan, ArmeniaK. S. MargaryanYerevan State Medical University after M. Heratsi, 0025, Yerevan, Armenia
2021en
ABI
Annotatsiya
Abstract A single-stage electrochemical synthesis of polymer complexes of Fe, Co, Ni, and Cu based on 1-vinyl-1,2,4-triazole has been elaborated. It has been found that 1-vinyl-1,2,4-triazole can be electropolymerized via the double bonds opening in the presence of potassium persulfate. At low current density, colored metal-polymer coatings have been formed at the surface of electrodes, and powders have been obtained at high current density. The composition and structure of the polymeric complexes have been elucidated by means of infrared spectroscopy, gas-liquid chromatography, elemental analysis, and thermogravimetric analysis.
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