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Synthesis of Carboxymethyl Starch for increasing drilling mud quality in drilling oil and gas wells

Konstantin M. MinaevTomsk Polytechnic University, 30 Lenina prospect, 634050, Tomsk, RussiaD. O. MartynovaTomsk Polytechnic University, 30 Lenina prospect, 634050, Tomsk, RussiaA. S. ZakharovTomsk Polytechnic University, 30 Lenina prospect, 634050, Tomsk, RussiaРашид Равильевич СагитовTomsk Polytechnic University, 30 Lenina prospect, 634050, Tomsk, RussiaA. BerTomsk Polytechnic University, 30 Lenina prospect, 634050, Tomsk, RussiaO S UlyanovaTomsk Polytechnic University, 30 Lenina prospect, 634050, Tomsk, Russia
2016en
ABI

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This paper describes the impact of carboxymethyl starch preparation conditions on physicochemical properties of polysaccharide reagent, widely used as fluid loss reducing agent in drilling mud. Variation of the main parameters of carboxymethylation is researched in the experiment. The following conditions such as temperature and reaction time, amount of water, as well as ratio of NaOH to monochloracetic acid define the characteristics of carboxymethyl starch. The degree of substitution is defined for polysaccharides, as well as the characteristics of samples have been studied by infrared spectroscopy. Rheological characteristics and fluid loss indicator have been investigated to study the impact of the reagents on drilling mud quality.

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