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Study of the pseudopolymorphism in the host–guest systems

Yu.I. ChumakovI nstitute of Applied Physics of Academy of Sciences of Moldova, 2028, Kishinev, Moldova,Elisabetta WeberInstitut fur Organische Chemie, Zechnische Universitat Bergakademie Freiberg, Germany,Б. Т. ИбрагимовS. A. TalipovMarilyn H. PerrinLaboratoire de cristallographie, CNRS, Universite Claude Bernard, LYON, France,Yu. A. SimonovInstitute of Applied PhysicsB. TashkhodjaevInstitute of Plant Substances Chemistry, Tashkent, Uzbekistan,
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Abstract

Supramolecular chemistry has opened a broad field of investigations to solid state physicists by its ability to produce new self-assembly materials [1]. A prototype tubular example of supramolecular self-organization is given by inclusion crystals, such as urea nanoporous compounds The host urea molecule forms hydrogen-bonded hexagonal channels of 5.5 diameter in which long guest chains like alkanes are densely packed in a one-dimensional arrangement. This simple paradigm crystal offers a unique opportunity to address at a fundamental level the question of the nature and the roles of interactions in self-organized architectures. Original physical properties in these host-guest materials are related to their aperiodic feature which, unambiguously, appears in their superspace diffraction pattern Here, we will present two quite new and unexpected results obtained in urea-alkane using neutron diffraction under Helium hydrostatic pressure: -the existence of a selective compressibility of the host and guest sublattice [4] -a total unexpected ordered phase where ordering does not require any apparent deformation of the host [5].

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