Article

8,13-Dimethylicosa-9,11-diyne-8,13-diol

Sarvinoz I. TirkashevaDepartment of Chemistry, Chirchik State Pedagogical University, A.Temur, 104, Chirchik 111700, UzbekistanOdiljon ZiyadullaevDepartment of Chemistry, Chirchik State Pedagogical University, A.Temur, 104, Chirchik 111700, UzbekistanVasiliy M. MuzalevskiyDepartment of Organic Chemistry, Moscow State University, Leninskiye Gory, 1, Moscow 119991, RussiaA.B. ParmanovDepartment of General and Oil-Gas Chemistry, National University of Uzbekistan, University Street, 4, Almazar District, Tashkent 100174, Uzbekistan

Molbankjournal2022en

ABI

Abstract

The protocol, 3-methyldec-1-yn-3-ol (1a) was chosen to perform the dimerization process. The optimal conditions for synthesis of 8,13-dimethylicosa-9,11-diyne-8,13 (2a) with high efficiency when using copper-catalyzed, N,N,N′N′-tetramethylethylenediamine as a ligand and CCl4 and methanol solvents in atmospheric pressure were determined. The structure of the obtained compound was proved by IR, 1H-NMR and 13C-NMR spectroscopy.

Topics

Natural product bioactivities and synthesis Microbial Natural Products and Biosynthesis Sesquiterpenes and Asteraceae Studies

Identifiers

DOI: 10.3390/m1484

Citations and references

Cited by 4 19 references

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