Nickel(II) complexes based on products of condensation of aroyl(perfluoroacyl)methanes with benzoylhydrazine
К. Г. АвезовBukhara State University, Bukhara, UzbekistanS. I. YakimovichSt. Petersburg State University, St. Petersburg, RussiaB. B. UmarovBukhara State University, Bukhara, UzbekistanВ. В. Пакальнис#R##N#St. Petersburg State UniversityГ.Г. АлександровKurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, Leninskii pr. 31, Moscow, 119991, RussiaT. N. NiyazkhanovBukhara State University, Bukhara, UzbekistanN. G. SevinchovBukhara State University, Bukhara, UzbekistanN.A. ParpievBukhara State University, Bukhara, Uzbekistan
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A series of novel complexes NiL n · NH3 were obtained by reactions of equimolar amounts of the ligands H2L n (prepared by condensation of aroyl(perfluoroacyl)methanes with benzoylhydrazine) as solutions in ethanol and nickel(II) acetate as a solution in aqueous ammonia. The empirical formulas and square planar structures of the complexes obtained were determined using elemental analysis, IR and 1H NMR spectroscopy, and X-ray diffraction.
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